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HCl (2.15 mL, 25.8 mmol) was slowly added into a stirred solution containing 3.5 g of (3R,5S)-6-(acetylthio)hexyl-4-acetamido-5-(tert-butoxycarbonylamino)-3-(pentan-3-yloxy)cyclohex-1-enecarboxylate (6) (6.5 mmol) dissolved in MeOH (30 mL) at room temperature, and then, the mixture was heated to 50 C