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Description

Le solide est ensuite filtr et lav avec de l'eau puis de l'thanol.0.065 g (-0.5 mmol per 1 iron per trimer) of iron (III) acetate (prepared according to the synthesis described in Example 1), 0.225 g of gadolinium (III) nitrate hexahydrate (0.5 mmol , Aldrich, 99.9%), 0.140 g of 1,3,5-benzenetricarboxylic acid (0.666 mmol, 95% Aldrich) dispersed in 10 ml of deionized water (or of methanol or ethanol or dimethylformamide), the all left 12 hours at 150 0 C in a Teflon body of 23 ml put in a metal bomb PAAR

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