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Except for the pyrolysis temperature, other conditions for the pyrolysis were kept the same in all experiments: purge time t = 0.0 s, equilibration time, t = 0.0 s, pyrolysis time 40 s, post pyrolysis time t = 12 s, valve temperature 250C, transfer line temperature 250C

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doi: 10.1038/tpj.2013.12 177